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caravan 89 repair manualReport this Document Download now Save Save Perkin Elmer Spectrum 2000 FTIR Manual.pdf For Later Perkin Elmer Spectrum 2000 FTIR Manual PDF Original Title: Perkin Elmer Spectrum 2000 FTIR Manual.pdf Uploaded by rbn.santiago 0 ratings 0 found this document useful (0 votes) 36 views 1 page More Save Save Perkin Elmer Spectrum 2000 FTIR Manual.pdf For Later 0 0 found this document useful, Mark this document as useful 0 0 found this document not useful, Mark this document as not useful Embed Share Print Download now Jump to Page You are on page 1 of 1 Search inside document Scribd members can read and download full documents. Your first 30 days are free. Continue Reading with Trial Share this document Share or Embed Document Sharing Options Share on Facebook, opens a new window Share on Twitter, opens a new window Share on LinkedIn, opens a new window Share with Email, opens mail client Copy Text Quick navigation Home Books Audiobooks Documents, active Footer menu Back to top About About Scribd Press Our blog Join our team. You can make a request for the operating manual by completing the adjoining form. Subsequently, you will receive the operating manual as pdf-file. Visit our Shop Request a PDF Therefore, you will receive offers and information about relevant topics by e-mail or post. You can unsubscribe from this notification at any time. This needs to be done every time the computer is turned back on. This will initialize the instrument and put it into a ready state. The Ready green LED light should be on after the instrument has initialized. Apparently, the ISA controller board does interact with the instrument to initialize it and put it into ready mode. Internal moisture will degrade the salt based piece inside the instrument. There's a help document on how to do this: File:Perkin Elmer Spectrum Changing the Transputer IO Address.doc.http://cnokorea.com/userfiles/entrypass-p1-server-user-manual.xml

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An application will be required to set the memory address of the transputer: D:\IR Spectroscopy Tools\Set Transputer IO Address.exe Also, the software will only work on Windows XP 32 bit edition. This software is installed in the CAL. Please upgrade to Internet Explorer version 10 or higher or install Google Chrome or Firefox to fully experience this site. Cord blood stem cells are doing amazing things. Learn More Ideally suited to everyday analysis, you can confidently perform fast, accurate IR analysis and assure the quality of your materials across a wide range of applications.True laboratory performance IR for everyday analysis is possible for everyone, everywhere. See the configurations table below for all available instrument options. Unique standardization allows data to be transferred precisely between instruments, side-by-side or in remote locations. The result is a complete solution to provide the fastest assurance of the quality of your materials, regardless of the application. Some of the industry applications that the Spectrum Two is designed to accommodate include: Spectrum Two is designed to function with a variety of “plug-and-go” sampling accessories to enhance the versatility of the instrument. We offer a range of UATR, HATR, Diffuse Reflectance, and Specular Reflectance accessories for use with the Spectrum Two system. The spectrometers can operate in ratio, single-beam, or interferogram mode. Designed for busy industrial or academic laboratories, this comprehensive FT-IR software package facilitates data collection, processing, and results generation. The software enables users without scientific training to generate infrared spectra from a sample and validate them against reference spectra in minutes, or even seconds.http://raynoxusa.com/raynoxusa/attach/entrypass-n2000-installation-manual.xml Spectrum 10 ES includes the comprehensive features of Spectrum 10 and encompasses user access control, audit trailing, data security, and data integrity to ensure secure analyses to meet the technical demands of 21 CFR Part 11 compliance. The simple user-installation and fast warm-up time means that the instrument can be set up quickly. The wide range of sampling accessories available can help your analysis move out of the laboratory. With optional features such as wireless connectivity to enable portable PC control, or the Portability Pack featuring a carrying case, battery pack, and 12V car auxiliary port adaptor, the Spectrum Two is ready to go where you go. One of the most important of these is alcohol-based hand sanitizer. To cope with this shortfall, the food and drug administration (FDA) has produced a guidance document for the compounding of certain alcohol-based hand sanitizer products. With many industries mobilizing to produce hand sanitizer for the first time, suppliers need quality control processes to ensure that the hand sanitizers produced are effective and safe. The physical and combustion properties of these biofuels have allowed them to achieve similar performance to diesel fuel. However, there are several characteristics that are of concern. These differences, especially the cetane reduction, require that adequate control of the biofuel concentration be implemented. Conventional methods such as microscopy and spectroscopy can be used to investigate the morphology and chemistry of a sample, but reveal little about its miscrostructure. The differing photosynthetic pathways in the plants used to produce these adulterants generally means that different techniques are required to detect them.As a result, insulating oil degrades over time, reducing its ability to act as an insulator and possibly leading to equipment failure. 2,6-di-tert-butyl-p-cresol (DBPC) and 2,6-di-tert-butyl phenol (DBP) are commonly used in transformer insulating oil as antioxidants. It is common practice for more antioxidant to be added if the level drops below 0.15. As a result of this, regular testing of transformer oils is necessary to ensure optimum functionality of transformer units. Infrared spectroscopy provides a fast method wherein the quantity of antioxidant in a sample may be determined in less than 30 seconds while adhering to regulations set out by ASTM D2668 and IEC 60666. This application note describes how the PerkinElmer Spectrum Two FT-IR spectrometer provides a fast, simple and cost-effective method for evaluating the levels of antioxidant in transformer insulating oil. The methodology followed for the analysis by FT-IR is reported in Bureau of Indian Standard and we have also tested for its ruggedness, spike recovery, linearity and detection limits. Oil and grease in water can cause surface films and shoreline deposits leading to environmental degradation, and can induce human health risks when discharge. FT-NIR spectroscopy provides rich information regarding the chemical composition of cannabis flower. When combined with chemometrics, the FT-NIR offers unparalleled speed and simplicity that cannot be matched by traditional techniques. PerkinElmer Spectrum Two NIR with the Near Infrared Reflectance Module (NIRM) is used to quantify total THC and total CBD in dried cannabis flower. The use of FT-NIR directly at the grow site would reduce overall research and development costs for cultivators. In this note we demonstrate that biodiesel from several common feedstocks can be distinguished on the basis of absorption bands arising from double bonds in the fatty acid chains. Verifying the FAME content of diesel-fuel blends is an important aspect of quality control and auditing of blending and distribution operations.It has many uses in the food, pharmaceutical and personal care industries due to its range of versatile properties allowing it to act as a sweetener, lubricant and humectant. Unscrupulous suppliers may adulterate glycerol to increase their profits. Diethylene glycol (DEG), the most common adulterant, has a number of properties similar to glycerol and is roughly three times cheaper. However, ingestion of DEG is toxic and thousands of reported cases of DEG poisoning have resulted in illness and fatalities worldwide. The current FDA safety limit for DEG in glycerol is 0.1 by weight. This study shows that using mid-infrared spectroscopy can detect DEG at that level. The PerkinElmer Spectrum Two FT-IR Spectrometer with UATR accessory provides a fast and robust method for determination of pharmaceutical packaging material. Furthermore, when used in conjunction with the Spectrum 10TM Enhanced Security, packaging can be easily analyzed while fulfilling requirements of 21 CFR part 11 compliance. The PerkinElmer Spectrum Two with the UATR accessory allows for the simple and rapid determination of cannabinoid concentrations in cannabis extract. The FT-IR-ATR technique offers a real-time solution to decarboxylation reaction monitoring. The ability to monitor this reaction over time would enable manufacturers of cannabis extract to optimize extraction conditions and identify process deviations. The FT-IR-ATR technique requires small sample quantities, zero sample preparation and minimal operator training. It can tell you the percentage of weight loss quantitatively and accurately. But TGA alone will not tell you anything about the chemical components of the evolved off gas. The hyphenation between TGA and FT-IR is able to identify the off gas from TGA and give a more complete picture of material characterization. The TG-IR hyphenation technique has been widely used for the polymer industry. This application note demonstrates how to combine the strength of TGA and FT-IR analysis to offers a more comprehensive material characterization. Broadly integrated into today’s industrial and commercial lifestyles, they make a major, irreplaceable contribution to virtually every product category. In this compendium you will find a wide range of applications for polymers, plastics, rubbers and advanced materials. Discover how to put these applications to work for you simply and efficiently. It is used extensively in the polymer, pharmaceutical, chemical, food, and electronics industries, to name a few, often identifying small contaminants or foreign objects of unknown origin. In forensic applications small particles of materials such as drugs, paint chips, residues or fibers are often collected as evidence and analyzed by IR microscopy.Biodiesel is one such renewable fuel. Rapeseed, soy, sunflower, palm and jatropha are just part of the range of feedstocks used globally in the production of biodiesel. To keep the focus on the riders and the bikes, the North West 200 requires each team to use a race-supplied control fuel. When it comes to testing, race organizers depend on highly accurate results within 10 minutes of sample collection. With that goal in mind, Euro M-Sport conducted exhaustive research on the available analytical options and instrumentation that would meet the specifications of the NW 200 fuel testing requirements. In response, we've gained years of experience developing a range of analytical capabilities to address a wide range of polymer analysis needs. Download the interactive brochure to learn more about the most common challenges and our solutions in the market. Powerful and adaptable, the Frontier meets all your current analysis needs and can be expanded as your research goals evolve. And with automated range switching, mid- near- or far-IR techniques are available at your fingertips. An exceptional signal-to-noise ratio and photometric performance assures optimal spectral performance to ensure best-in-class sensitivity. This configurable platform provides dependable, consistent and trouble-free operation through years of service. But how else does one describe a laboratory instrument that will dramatically improve the understanding of materials across an unprecedented range of industries. It is quite simply the most productive laboratory FT-IR imaging system in the world. Historically, operational budgets have been limited and with intermittent use, universities could not justify the purchase. Adding value to Western Norway’s educational program, the Avio 200 provides students with the opportunity to develop relevant analytical skills. Combined with the low argon consumption while in operation resulting from the flat-plate design, the Avio 200 is the perfect instrument for universities to use in both teaching and research scenarios. Evolved Gas Analysis (EGA) solutions combine multiple analytical technologies to empower speed and advanced information acquisition. This comprehensive technology guide is your guide to understanding how hyphenation provides the insights - not just WHEN something has happened, but also WHAT happened. There is more and more pressure to achieve high product quality and reduce costs in order to stay one step ahead of the competition. Not only does plastic recycling reduce environmental problems caused by polymeric waste accumulation, it will also lead to a decrease in oil consumption and green-house gas emissions. The PerkinElmer Recycling Packages make use of the most commonly used techniques for material characterization and additionally supports the Plastic Identification Codes (PIC), used worldwide for packaging applications. Designed for novice and advanced spectroscopists who need to integrate accurate quantitative analysis into their IR or NIR analysis. The technique requires good contact between the sample and a crystal made from a material which transmits IR radiation and has a high refractive index. Consequently it is widely used for attenuated total reflectance (ATR) and liquid transmission cells. Complete, consistent, and accurate data should be attributable, legible, contemporaneously recorded, original or a true copy, and accurate (ALCOA)”. ALCOA itself has evolved to ALCOA Plus, which incorporates two of the fundamental definition terms as stated by the FDA; complete, consistent, enduring, and available. Compliance with 21 CFR Part 11 is mandatory for pharmaceutical companies and their suppliers to sell products into the United States, and also applies to other related industries. It affords the system owner the ability to comply with regulations and incorporate features into the validation plan to exhibit compliance. The purpose of this document is to demonstrate how Spectrum 10 ES meets the technical requirements for 21 CFR Part 11. Learn More. Learn More Some common applications for molecular spectroscopy study in the near, near-mid, mid-far and far infrared regions include: The highly configurable platform provides dependable, consistent, and trouble-free operation through years of service.Polymer ID Analyzer from PerkinElmer is a compact and easy-to-use solution designed to simplify and accelerate your polymer analysis. Quickly and confidently identify unknown polymer samples, determine composition of blends, and verify quality.Remarkably easy to use, you can be confident in generating consistent quality spectra. Ideally suited to everyday analysis, you can confidently perform fast, accurate IR analysis and assure the quality of your materials across a wide range of applications.Compact, robust, and completely transportable, samples can be run on the Spectrum Two either in the laboratory or out in the field. It is used to secure the components of the assembled cell in place. This set comes with the Evacuable Die, but it can also be ordered separately as a replacement or spare part. Each half has a CaF 2 window.Please note: When rectangular windows and spacers are used, the Universal Demountable Cell becomes a Semi-Demountable Cell. It comes pre-aligned and ready to install.The mini-press requires, but does not include the holder (51002593). A KBr pellet is formed in the metal collar that fits into the Pellet Holder (51002593), which is a required component of the quick press, but is not included with the accessory. Learn More Renowned for their sensitivity, spatial resolution, ease of use, and results, they’re engineered to the highest quality specifications and ISO-9000 standards and deliver the highest levels of throughput, reproducibility, and accuracy. So you’re able to analyze even the smallest sample with pinpoint precision. It’s also one of the easiest to use, even for nonprofessionals, with no (or minimal) manual adjustments necessary. And you can even get unattended operation if you need it. Nothing could be simpler. The device identifies materials, impurities, detects functionalities or determines optical properties (refraction index, extinction coefficient) of films and compact solid states within the ultra-red spectroscopic range. And by having access to our ebooks online or by storing it on your computer, you have convenient answers with Viewcontent Php3Farticle3Dperkin Elmer Diamond Manual26context3Dlibpubs. To get started finding Viewcontent Php3Farticle3Dperkin Elmer Diamond Manual26context3Dlibpubs, you are right to find our website which has a comprehensive collection of manuals listed. Our library is the biggest of these that have literally hundreds of thousands of different products represented. I get my most wanted eBook Many thanks If there is a survey it only takes 5 minutes, try any survey which works for you. In 2005, the instrument was upgraded to a Bruker Tensor37 funded by a A. Conly- CFI grant. Equipment: Bruker Tensor 37 Fourier Transform Infrared Spectrophotometer. Bruker Hyperion 2000- IR Microscope with 4x, 15x and 36x objectives and polarizer. NIR Source InGaAs Detector 12.8-5.8 K Auto mirror selector CAF2 10- 1.650 Cm-1 beam splitter OPUS site licence for Lakehead University. ATR (attenuated total reflectance) and diffuse reflectance accessories including Pike MIRacel with ZnSe crystal and with ATR-Ge objective (20x) for the IR microscope Hydraulic press for KBr disk production Spectral libraries, search and match software (Sadtler IR-SearchMaster 6.0, FIveash-Polymer and Mineral), functional group database. Citations are the number of other articles citing this article, calculated by Crossref and updated daily. Find more information about Crossref citation counts. The Altmetric Attention Score is a quantitative measure of the attention that a research article has received online. Clicking on the donut icon will load a page at altmetric.com with additional details about the score and the social media presence for the given article. Find more information on the Altmetric Attention Score and how the score is calculated. Learn More Login with ACS ID Please reconnect By continuing to use the site, you are accepting our use of cookies. Read the ACS privacy policy. The cable for connecting our Spectrum 2000 FTIR spectrometer to a computer is missing. Do you know if it would be possible for me to connect a PC to the instrument using an Ethernet cable? Does the manual specifiy that the connection is Ethernet? I also seriously doubt this is ethernet. It is either serial or it connects to a custom interface board plugged into the motherboard (ISA, PCI, etc). It won't be ethernet.;D I apologise for posting my technical question in the wrong place! Looks like a circular male connector (6 contacts).I'll try to get hold of the correct connectors so that I can hopefully link the instrument to a PC! Looks like a circular male connector (6 contacts).I'll try to get hold of the correct connectors so that I can hopefully link the instrument to a PC! Do you have any software to control the instrument? All rights reserved. This IR probe has a spectral range of 5000-cm -1 to 900cm 1 The difference in emission intensities released perpendicular to the excitation light is then measured for the sample, and the temperature scan data and spectrum are obtained and displayed. FTIR may also refer to Frustrated total internal reflection. An FTIR spectrometer simultaneously collects high-resolution spectral data over a wide spectral range. This confers a significant advantage over a dispersive spectrometer, which measures intensity over a narrow range of wavelengths at a time.Rather than shining a monochromatic beam of light (a beam composed of only a single wavelength) at the sample, this technique shines a beam containing many frequencies of light at once and measures how much of that beam is absorbed by the sample. Next, the beam is modified to contain a different combination of frequencies, giving a second data point. This process is rapidly repeated many times over a short time span. Afterwards, a computer takes all this data and works backward to infer what the absorption is at each wavelength.The light shines into a Michelson interferometer —a certain configuration of mirrors, one of which is moved by a motor. As this mirror moves, each wavelength of light in the beam is periodically blocked, transmitted, blocked, transmitted, by the interferometer, due to wave interference. Different wavelengths are modulated at different rates, so that at each moment or mirror position the beam coming out of the interferometer has a different spectrum.The processing required turns out to be a common algorithm called the Fourier transform.Later instruments used potassium bromide prisms to extend the range to 25 ?m (400 cm ?1 ) and caesium iodide 50 ?m (200 cm ?1 ). The region beyond 50 ?m (200 cm ?1 ) became known as the far-infrared region; at very long wavelengths it merges into the microwave region. Measurements in the far infrared needed the development of accurately ruled diffraction gratings to replace the prisms as dispersing elements, since salt crystals are opaque in this region. More sensitive detectors than the bolometer were required because of the low energy of the radiation. One such was the Golay detector. An additional issue is the need to exclude atmospheric water vapour because water vapour has an intense pure rotational spectrum in this region. Far-infrared spectrophotometers were cumbersome, slow and expensive. The advantages of the Michelson interferometer were well-known, but considerable technical difficulties had to be overcome before a commercial instrument could be built. Also an electronic computer was needed to perform the required Fourier transform, and this only became practicable with the advent of mini-computers, such as the PDP-8, which became available in 1965.Ideally 50 of the light is refracted towards the fixed mirror and 50 is transmitted towards the moving mirror. Light is reflected from the two mirrors back to the beam splitter and some fraction of the original light passes into the sample compartment. There, the light is focused on the sample. On leaving the sample compartment the light is refocused on to the detector. The difference in optical path length between the two arms to the interferometer is known as the retardation or optical path difference (OPD). An interferogram is obtained by varying the retardation and recording the signal from the detector for various values of the retardation. The form of the interferogram when no sample is present depends on factors such as the variation of source intensity and splitter efficiency with wavelength. The position of zero retardation is determined accurately by finding the point of maximum intensity in the interferogram. When a sample is present the background interferogram is modulated by the presence of absorption bands in the sample.Common to all these arrangements is the need to ensure that the two beams recombine exactly as the system scans. The simplest systems have a plane mirror that moves linearly to vary the path of one beam. In this arrangement the moving mirror must not tilt or wobble as this would affect how the beams overlap as they recombine. Some systems incorporate a compensating mechanism that automatically adjusts the orientation of one mirror to maintain the alignment. Arrangements that avoid this problem include using cube corner reflectors instead of plane mirrors as these have the property of returning any incident beam in a parallel direction regardless of orientation.One common system incorporates a pair of parallel mirrors in one beam that can be rotated to vary the path without displacing the returning beam. Another is the double pendulum design where the path in one arm of the interferometer increases as the path in the other decreases.One limitation of this approach is that the variation of refractive index over the wavelength range limits the accuracy of the wavelength calibration.In practice the scan can be on either side of zero resulting in a double-sided interferogram. Mechanical design limitations may mean that for the highest resolution the scan runs to the maximum OPD on one side of zero only.This requires it to be stored in digital form as a series of values at equal intervals of the path difference between the two beams. To measure the path difference a laser beam is sent through the interferometer, generating a sinusoidal signal where the separation between successive maxima is equal to the wavelength of the laser (typically a 633 nm HeNe laser is used). This can trigger an analog-to-digital converter to measure the IR signal each time the laser signal passes through zero.The range of wavelengths that can be used in the calculation is limited by the separation of the data points in the interferogram. The shortest wavelength that can be recognized is twice the separation between these data points. The wavelengths used in calculating the Fourier transform are such that an exact number of wavelengths fit into the length of the interferogram from zero to the maximum OPD as this makes their contributions orthogonal. This results in a spectrum with points separated by equal frequency intervals. The corresponding frequencies are ? 1 and ? 2:For example, a maximum OPD of 2 cm results in a separation of 0.5 cm ?1. This is the spectral resolution in the sense that the value at one point is independent of the values at adjacent points. Most instruments can be operated at different resolutions by choosing different OPD's. Instruments for routine analyses typically have a best resolution of around 0.5 cm ?1, while spectrometers have been built with resolutions as high as 0.001 cm ?1, corresponding to a maximum OPD of 10 m. The point in the interferogram corresponding to zero path difference has to be identified, commonly by assuming it is where the maximum signal occurs. This so-called centerburst is not always symmetrical in real world spectrometers so a phase correction may have to be calculated. The interferogram signal decays as the path difference increases, the rate of decay being inversely related to the width of features in the spectrum. If the OPD is not large enough to allow the interferogram signal to decay to a negligible level there will be unwanted oscillations or sidelobes associated with the features in the resulting spectrum. To reduce these sidelobes the interferogram is usually multiplied by a function that approaches zero at the maximum OPD. This so-called apodization reduces the amplitude of any sidelobes and also the noise level at the expense some reduction in resolution.A string of zeroes may be added to the measured interferogram to achieve this. More zeroes may be added in a process called zero filling to improve the appearance of the final spectrum although there is no improvement in resolution.This arises from the fact that information from all wavelengths is collected simultaneously. It results in a higher signal-to-noise ratio for a given scan-time for observations limited by a fixed detector noise contribution (typically in the thermal infrared spectral region where a photodetector is limited by generation-recombination noise ). For a spectrum with m resolution elements, this increase is equal to the square root of m. Alternatively, it allows a shorter scan-time for a given resolution. In practice multiple scans are often averaged, increasing the signal-to-noise ratio by the square root of the number of scans. This results from the fact that in a dispersive instrument, the monochromator has entrance and exit slits which restrict the amount of light that passes through it. The interferometer throughput is determined only by the diameter of the collimated beam coming from the source. Although no slits are needed, FTIR spectrometers do require an aperture to restrict the convergence of the collimated beam in the interferometer. This is because convergent rays are modulated at different frequencies as the path difference is varied.The wavelength scale is calibrated by a laser beam of known wavelength that passes through the interferometer. This is much more stable and accurate than in dispersive instruments where the scale depends on the mechanical movement of diffraction gratings. In practice, the accuracy is limited by the divergence of the beam in the interferometer which depends on the resolution. In dispersive instruments, this is the result of imperfections in the diffraction gratings and accidental reflections.